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33 changes: 33 additions & 0 deletions cif_pow.dic
Original file line number Diff line number Diff line change
Expand Up @@ -12140,6 +12140,37 @@ save_PD_SPEC
_name.category_id PD_GROUP
_name.object_id PD_SPEC
_category_key.name '_pd_spec.id'
_description_example.case
;
_pd_spec.prep_id ABC123_main
_pd_spec.id ABC123_03
_pd_spec.description 'Iron ore from FeOre Inc. ID number ABC123'
_pd_spec.mount_mode reflection
_pd_spec.mounting 'back-packed powder pellet'
_pd_spec.orientation horizontal
_pd_spec.preparation
;
50 g of received sample was homogenised and cone-and-quartered
to obtain a 3 g split. 1 g of ɑ-alumina was added as an internal
standard. The specimen was micronised for 15 min with 15 ml of
ethanol and dried at 45 °C. The resulting powder was backpressed
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into a holder with a semi-automated press.
;
_pd_spec.shape flat_sheet
_pd_spec.size_axial 25.0
_pd_spec.size_equat 25.0
_pd_spec.size_thick 3.5
;
_description_example.detail
;
A specimen of iron ore, from FeOre Inc., with an added internal
standard was prepared for analysis. The sample from which the specimen
was prepared is identified by a _pd_prep.id values of "ABC123_main".
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The data were collected in reflection on an instrument where the
incident and diffracted beams are vertical. The specimen flat, and is
25.0 x 25.0 mm, or it could be inferred to be 25 mm diameter.
The specimen was prepared as described.
;

save_

Expand Down Expand Up @@ -12830,4 +12861,6 @@ save_
Updated descriptions of data items linked to _pd_data.point_id to
clarify that identical values refer to the same data point in each
disparate loop; they cannot be assigned values independently.

Added example PD_SPEC
;