diff --git a/cif_pow.dic b/cif_pow.dic index c69bd1f..3ce49ab 100644 --- a/cif_pow.dic +++ b/cif_pow.dic @@ -7900,7 +7900,7 @@ save_PD_INSTR_DETECTOR _definition.id PD_INSTR_DETECTOR _definition.scope Category _definition.class Loop - _definition.update 2023-01-06 + _definition.update 2025-06-19 _description.text ; This category contains information relevant to the detector @@ -7927,6 +7927,79 @@ save_PD_INSTR_DETECTOR _name.object_id PD_INSTR_DETECTOR _category_key.name '_pd_instr_detector.id' + loop_ + _description_example.case + _description_example.detail +; + loop_ + _pd_instr_detector.id + _pd_instr.dist_spec_detc + _pd_instr.slit_ax_spec_detc + _pd_instr.slit_eq_spec_detc + _pd_instr_detector.instr_id + fd343493 320 8.5 0.075 b4131be5 + 47540661 320 8.5 0.075 b4131be5 +; +; + These detectors are paired with the instrument identified by the + id b4131be5. + + There are two detectors, fd343493 and 47540661. Both detectors are + positioned 320 mm from the specimen, and are defined by two slits, + 8.5 mm in the axial direction, and 0.075 mm in the equatorial direction. + As the detector window is 8.5 mm wide, with 75 μm wide pixels, this is + represented by _pd_instr.slit_eq_spec_detc as 0.075 and + _pd_instr.slit_ax_spec_detc as 8.5 +; +; + _pd_instr_detector.id WhizzBang + _pd_instr_detector.instr_id 58b6d83b + _pd_instr.2theta_monochr_post 31.0 + _pd_instr.dist_anal_detc 47 + _pd_instr.dist_spec_anal 135 + _pd_instr.monochr_post_spec 'Graphite mosaic monochromator' + _pd_instr.slit_ax_spec_anal 9.5 + _pd_instr.slit_eq_spec_anal 0.5 + _pd_instr.soller_eq_spec_anal 2.5 + _pd_instr.special_details + ; + The equatorial slit between the specimen and monochromator + lies on the detector circle. + ; +; +; + The 'WhizzBang' detector is paired with the instrument identified by the + id 58b6d83b. + + The post-specimen, graphite, mosaic monochromator is set at 31.0° 2θ. + The monochromator is situated 47 mm from the detector. The distance from + the specimen to the monochromator is 135 mm. The width of the beam is + defined at the monochromator by a 9.5 mm mask. There is a 0.5 mm + equatorial slit on the detector circle between the specimen and + monochromator, which acts as the virtual detector. There are 2.5° axial + Soller slits between the specimen and the monochromator. +; +; + _pd_instr_detector.instr_id 58b6d83b + _pd_instr_detector.id A + _pd_instr.dist_spec_detc 117.5 + _pd_instr.monochr_post_spec 'Fe filter' + _pd_instr.slit_ax_spec_detc 12 + _pd_instr.slit_eq_spec_detc 0.075 + _pd_instr.soller_ax_spec_detc 2.5 +; +; + The 'A' detector is paired with the instrument identified by the + id 58b6d83b. + + The distance from the specimen to the detector is 117.5 mm. The X-ray + beam is "monochromatised" by a metal Fe filter. The detector is defined + by a 12 mm axial and 0.075 mm equatorial slit. The small size of the + equatorial slit might lead the reader to assume a strip detector was + used. This should be documented using _pd_instr.special_details. There + are 2.5° axial Soller slits between the specimen and the detector. +; + save_ save_pd_instr.2theta_monochr_post @@ -14330,9 +14403,11 @@ save_ clarify that identical values refer to the same data point in each disparate loop; they cannot be assigned values independently. + Added _pd_instr_detector.instr_id + Added examples to PD_CALC_OVERALL, PD_CALIB_INCIDENT_INTENSITY, PD_CHAR, - PD_DIFFRACTOGRAM, PD_INSTR, PD_MEAS_OVERALL, PD_PEAK, _pd_phase.id, - PD_PHASE_MASSS, PD_PREP, PD_PROC_LS, PD_PROC_OVERALL, + PD_DIFFRACTOGRAM, PD_INSTR, PD_INSTR_DETECTOR, PD_MEAS_OVERALL, PD_PEAK, + _pd_phase.id, PD_PHASE_MASS, PD_PREP, PD_PROC_LS, PD_PROC_OVERALL, PD_QPA_CALIB_FACTOR, PD_QPA_INTENSITY_FACTOR, PD_QPA_INTERNAL_STD, PD_SPEC.